96 Line高温大容量同步热分析/热重分析-气体联用分析仪

技术特点

Large volume & high temperature TGA/STA-EGA (ambient to 2000°C)

This is an extremely high performance weighing module used with the TGA 96. This balance can weigh samples up to 100 g and is well suited to measuring both micro-quantities of samples (a few milligrams) as well as large, dense samples while maintaining measurement resolution to within a microgram whatever the mass analyzed. 96 Line TGA/STA offers EGA temperature controlled coupling devices, enabling simultaneous heated capillary based MS, or GC/MS* connections

Simultaneous TGA-DTA/DSC measurements are available.

Simultaneous TGA-DTA: – Ambient to 1600°C, – Ambient to 1750°C, – Ambient to 2000°. Simultaneous TGA-DSC: – Ambient to 1500°C, – Ambient to 1600°C.

NEW PARTS AND OPTIONS
Pierced alumina crucibles
Alumina based crucibles pierced with numerous orifices to improve sample / gas interactions are available. 18mL and 4.5mL versions are available.

FTIR coupling
A heated MS or FTIR 200°C coupling was designed for the TG96 line.

技术参数
96 Line DTA 96 DSC 96 TGA
Temperature range of measurement module (C°) amb/1600, amb/1750, amb/2000 amb/1500, amb/1600 amb/1600, amb/1750, amb//2000
Volume of crucible (μl) 220/550 360/420 18000
Max. sample size(mm) n/a n/a n/a
Resolution n/a 5μW 0.3 μg
RMS noise n/a 66 μW 0,3 μg
Specific RMS noise n/a 0,16 μW/μl 0,016μg/ml
Measurement range n/a n/a +/-2000 mg
Evolved Gas Analysis Simultaneous MS, GC/MS*Thermostated interfaces up to 300°C
特征

In addition to the TGA 96, SETARAM proposes different accessories and software that permit, in particular:
– TGA measurements in corrosive atmospheres
– Controlled rate TGA measurement (CRTA: controlled rate thermal analysis)

Evolved Gas Analysis

96 Line offers temperature controlled coupling devices, enabling simultaneous MS, or GC/MS* connections. The coupling device is heated up to 200°C to avoid gas condensation and is completely insulated for a safe handling. 96 Line can be equipped on request with the state-of-the-art heated “Autoinjector” interface for TG-GC/MS* experiments.

*GC/MS is available on request.

应用案例
Typical application area Materials
Gasification, pyrolysis, combustion Coal, biomass and wastes
Adsorption, desorption, calcination Catalysts, sorbents, minerals
Dehydration, dehydroxylation, decarbonatation Cements, minerals, ceramics, pharmaceuticals
Thermal stability, compositional analysis Pharmaceuticals, polymers, cements, minerals, ceramics
Oxidation Metals, alloys
Residual solvents Pharmaceuticals
Polycondensation, curing Polymers
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TGA/STA-GC/MS : 96 Line高温大容量同步热分析/热重分析-气体联用分析仪 par SETARAM